ENSTRÜMANTEL ANALİZ PROGRAMME COURSE DESCRIPTION

Code	Name of the Course Unit	Semester	In-Class Hours (T+P)	Credit	ECTS Credit
LTP154	ENSTRÜMANTEL ANALİZ	2	2	2	7

GENERAL INFORMATION
Language of Instruction :	Turkish
Level of the Course Unit :	ASSOCIATE DEGREE, TYY: + 5.Level, EQF-LLL: 5.Level, QF-EHEA: Short Cycle
Type of the Course :	Compulsory
Mode of Delivery of the Course Unit	-
Coordinator of the Course Unit	Assist.Prof. SEÇİL KIRLANGIÇ ATAŞEN
Instructor(s) of the Course Unit	Assist.Prof. SEÇİL KIRLANGIÇ ATAŞEN
Course Prerequisite	No

OBJECTIVES AND CONTENTS
Objectives of the Course Unit:	This course aims to teach the fundamental principles of spectroscopic, chromatographic, and electroanalytical instrumental analysis methods; the basic components, characteristics, and operating principles of the instruments used; to provide knowledge on the analytical applications of these methods; and to enable students to interpret analytical outputs in order to perform substance analyses.
Contents of the Course Unit:	The course covers an introduction to instrumental analysis; radiation and its properties; the electromagnetic wave spectrum; interaction of light with matter; spectroscopy; spectrophotometers and their components; atomic absorption spectrometry; atomic emission spectrometry; ultraviolet–visible molecular absorption spectrometry; calibration in instrumental methods; turbidimetry; refractometry; polarimetry; molecular luminescence spectrometry (fluorescence and phosphorescence); general concepts of chromatography; chromatographic methods; mass spectrometry; and electroanalytical methods.

KEY LEARNING OUTCOMES OF THE COURSE UNIT (On successful completion of this course unit, students/learners will or will be able to)
Defines the basic concepts of electromagnetic radiation.
Defines the fundamental concepts of instrumental analysis methods.
Lists the basic components of instrumental analysis instruments.
Explains the basic principles of spectrometric methods.
Compares the instruments used in spectrometric methods.
Explains the basic principles of chromatographic separation methods.
Classifies the instruments and materials used in chromatographic methods.
Interprets qualitative and quantitative analysis results.
Constructs a calibration curve step by step.
Calculates absorbance values using the Lambert–Beer Law.
Defines the basic concepts related to electroanalytical methods.

WEEKLY COURSE CONTENTS AND STUDY MATERIALS FOR PRELIMINARY & FURTHER STUDY
Week	Preparatory	Topics(Subjects)	Method
1	Literature review, individual research.	Defines the Basic Concepts of Electromagnetic Radiation	Expression, video, question and answer
2	Literature review, individual research.	Introduction to instrumental analysis, Beam and its properties, electromagnetic wave spectrum, Interaction of light with matter	Expression, video, question and answer
3	Literature review, individual research.	Atomic Absorption Spectrometry	Expression, video, question and answer
4	Literature review, individual research.	Atomic Emission Spectrometry	Expression, video, question and answer
5	Literature review, individual research.	Ultraviolet-Visible Molecular Absorption Spectrometry	Expression, video, question and answer
6	Literature review, individual research.	Calibration in Instrumental Methods	Expression, video, question and answer
7	Literature review, individual research.	Turbidimetry, Refractometry, Polarimetry	Expression, video, question and answer
8	Literature review, individual research.	Molecular Luminescence Spectrometry (Fluorescence and phosphorescence)	Expression, video, question and answer
9	Literature review, individual research.	General information about Chromatography	Expression, video, question and answer
10	-	MID-TERM EXAM	-
11	Literature review, individual research.	Chromatographic Methods (Thin Layer Chromatography (TLC), High Pressure Liquid Chromatography (HPLC)	Expression, video, question and answer
12	Literature review, individual research.	Chromatographic Methods (Gas Chromatography (GC), Column Chromatography)	Expression, video, question and answer
13	Literature review, individual research.	Mass Spectrometry, GC-MS- HPLC-MS	Expression, video, question and answer
14	Literature review, individual research.	Electroanalytical Methods (Coulometry, Potentiometry)	Expression, video, question and answer
15	Literature review, individual research.	Voltammetry	Expression, video, question and answer
16	-	FINAL EXAM	-
17	-	FINAL EXAM	-

SOURCE MATERIALS & RECOMMENDED READING
Skoog, D. A. ,F.J. Holler, T.A. Nieman, (Çev:E. Kılıç) (2013). Enstrümantal Analiz, 6.Baskı, Bilim Yayıncılık, Ankara.
Bağ H ve ark. (2017). Analitik Kimya, 6. Baskı, Pegem Akademi, Ankara.
Skoog, D. A., F.J. Holler, T.A.,West D. M., Holler F.J. Fundamentals of Analytical Chemistry, Ninth Edition, Mary Finch, USA.
Gamlı F, (2016). Laboratuvar Teknikleri ve Temel Gıda Analizleri, 3.Baskı, Dora Yayıncılık, Bursa.

ASSESSMENT
Assessment & Grading of In-Term Activities	Number of Activities	Degree of Contribution (%)	Description	Examination Method

Level of Contribution
0	1	2	3	4	5

KNOWLEDGE
Theoretical
	Programme Learning Outcomes	Level of Contribution
		0	1	2	3	4	5
1	Explains the basic concepts of mathematics and natural sciences.				3
2	Defines the basic concepts and theoretical knowledge used in laboratories.					4
3	Explains the properties and operating principles of instruments, materials, and chemicals used in laboratories.				3

KNOWLEDGE
Factual
	Programme Learning Outcomes	Level of Contribution
		0	1	2	3	4	5
1	Has knowledge of current laboratory practices, scientific literature, and emerging technologies.						5
2	Explains laboratory safety and occupational health principles in a systematic manner.			2
3	Explains national and international standards used in laboratory fields in detail.				3

SKILLS
Cognitive
	Programme Learning Outcomes	Level of Contribution
		0	1	2	3	4	5
1	Evaluates the data collected through sampling, experimentation, and analysis processes.						5
2	Interprets the data obtained from laboratory instruments on a scientific basis.						5

SKILLS
Practical
	Programme Learning Outcomes	Level of Contribution
		0	1	2	3	4	5
1	Uses laboratory equipment and tools appropriate for the experiment effectively.					4
2	Prepares solutions required for experimental studies using accurate calculations.						5
3	Applies modern laboratory methods used in food, water, plant–soil, and medical analyses.						5
4	Determines the chemical, physical, and biological properties of samples (food, water, medical, soil, and plant) using various analytical methods.						5
5	Uses chemical substances in accordance with safety rules and occupational health and safety regulations.					4

OCCUPATIONAL
Autonomy & Responsibility
	Programme Learning Outcomes	Level of Contribution
		0	1	2	3	4	5
1	Communicates effectively with the laboratory team by supporting teamwork and interdisciplinary collaboration.		1

OCCUPATIONAL
Learning to Learn
	Programme Learning Outcomes	Level of Contribution
		0	1	2	3	4	5
1	Demonstrates awareness of the importance of lifelong learning by keeping up with developments in science and technology and continuously improving oneself.				3

OCCUPATIONAL
Communication & Social
	Programme Learning Outcomes	Level of Contribution
		0	1	2	3	4	5
1	Acts in accordance with professional ethical principles.						5

OCCUPATIONAL
Occupational and/or Vocational
	Programme Learning Outcomes	Level of Contribution
		0	1	2	3	4	5
1	Applies laboratory safety and emergency procedures during work processes.		1
2	Uses techniques related to laboratory technology and laboratory instruments, equipment, and devices appropriately and effectively.					4
3	Performs analyses of food, water, plant, soil, chemical, microbiological, and medical materials.						5

WORKLOAD & ECTS CREDITS OF THE COURSE UNIT
Workload for Learning & Teaching Activities
Type of the Learning Activites	Learning Activities (# of week)	Duration (hours, h)	Workload (h)
Lecture & In-Class Activities	14	2	28
Preliminary & Further Study	14	2	28
Land Surveying	0	0	0
Group Work	0	0	0
Laboratory	0	0	0
Reading	14	4	56
Assignment (Homework)	0	0	0
Project Work	0	0	0
Seminar	0	0	0
Internship	0	0	0
Technical Visit	0	0	0
Web Based Learning	0	0	0
Implementation/Application/Practice	0	0	0
Practice at a workplace	0	0	0
Occupational Activity	0	0	0
Social Activity	0	0	0
Thesis Work	0	0	0
Field Study	0	0	0
Report Writing	0	0	0
Final Exam	1	1	1
Preparation for the Final Exam	2	15	30
Mid-Term Exam	1	1	1
Preparation for the Mid-Term Exam	2	15	30
Short Exam	2	1	2
Preparation for the Short Exam	0	0	0
TOTAL	50	0	176